The Project NOLEAD - Motivation
International efforts in removing toxic substances from everyday applications are increasing.
The EU passed the "Waste Electrical and Electronic Equipment" (WEEE) and "Restriction of the use of certain
Hazardous Substances in electrical and electronic equipment" (RoHS) in 2003[1].
While the WEEE regulates the disposal, reuse and recycling of the mentioned equipment, the RoHS is a necessary
requirement to ensure this can be accomplished safely without endangering the environment or people´s health.
Mercury, cadmium, hexavalent chromium, the flame-retardants PBB and PBDE and, the focus of this work, lead, have
been identified as a primary risk during recycling, disposal or just improper use.
Therefore, as of June 2006, any products introduced to the open market may not include more than 0.1 wt.% of any one
of these substances with the exception of cadmium where the limit is even lower than 0.01 wt.%. Currently, an exemption
is made for piezoelectrics. However, known lead-free piezoceramics are not yet good enough to replace lead containing
materials. While this exemption currently holds for almost all piezoelectric components on the market, this is subject
to regular review. New applications using these materials can only be introduced if "elimination or substitution ... is
technically or scientifically impracticable, or where the negative environmental, health and/or consumer safety impacts
caused by substitution are likely to outweigh the environmental, health and/or consumer safety benefits"[1].
This would for example likely not hold for the use of lead in newly invented consumer electronics.
It is, therefore, desirable to find alternatives to the currently market-dominating lead containing piezoelectrics
in all current or future applications.
A significant research effort into lead-free alternatives to PZT began a little over ten years ago even though the
base materials have been known for more than half a century[2,3]. The research activities before 1990 mostly aimed at
searching for the systems, whose properties are better than those of PZT. Increased Curie temperature or polarisation
is often desirable for example. However, this was not meant for environmental protection but merely a search for the
systems with improved properties over PZT. Since about 1990, the search has mostly directed to
improving the already known lead-free materials to the point where they might reach PZT-like properties due to
before-mentioned legislation.
In this project we study sodium potassium niobate (NKN) with the aim to replace PZT in future
piezoelectric/ferroelectric devices. The thin films are realised via Pulsed Laser Deposition.
References:
- "EU-Directive 2002/95/EC: Restriction of the use of certain hazardous substances in electrical
and electronic equipment (RoHS)," Official Journal of the European Union, 46[L37] 19-23 (2003).
- L. Egerton and D. M. Dillon, "Piezoelectric and dielectric properties of ceramics in the system potassium sodium
niobate," Journal of the American Ceramic Society, 42[9] 438-42 (1959)
- G. A. Smolenskii and A. I. Agranovskaya, "Dielectric Polarization of a Number of Complex Compounds,"
Soviet Physics-Solid State, 1[10] 1429-37 (1960)